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  4. Spray drying of energetic materials at the example of Octogen
 
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June 2023
Conference Paper
Title

Spray drying of energetic materials at the example of Octogen

Abstract
Particle properties such as size, morphology and purity are important for propellant, explosive, and pyrotechnic formulations. The focus of this work was to produce high energy explosives particles with these properties. The spray drying method was used to prepare 1,3,5,7-tetranitro-1,3,5,7-tetrazocane (HMX) particles.
Particle size analysis showed that HMX particles in a size range from 0.4 µm to 15 µm can be produced with the spray drying equipment available at Fraunhofer ICT. Scanning electron microscope (SEM) images also showed that it is possible to produce spherical particles. Furthermore, the spray-dried particles were investigated crystallographically. X-ray powder diffraction (XRD) showed that the HMX particles consist of the β-HMX.
Author(s)
Busch, Konstantin  
Fraunhofer-Institut für Chemische Technologie ICT  
Herrmann, Michael  
Fraunhofer-Institut für Chemische Technologie ICT  
Maier, Marko
Fraunhofer-Institut für Chemische Technologie ICT  
Heintz, Thomas  orcid-logo
Fraunhofer-Institut für Chemische Technologie ICT  
Mainwork
Energetic Materials - Analysis, Characterization, Modelling  
Conference
Fraunhofer-Institut für Chemische Technologie (International Annual Conference) 2023  
Language
English
Fraunhofer-Institut für Chemische Technologie ICT  
Keyword(s)
  • Spray drying

  • HMX

  • Octogen

  • 1,3,5,7-Tetranitro-1,3,5,7-tetrazocan

  • X-ray powder diffraction

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