Fraunhofer-Institut für Zuverlässigkeit und Mikrointegration IZM

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  • Publication
    Experimental and computational studies on the role of surface functional groups in the mechanical behavior of interfaces between single-walled carbon nanotubes and metals
    ( 2016)
    Hartmann, S.
    ;
    Sturm, H.
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    Blaudeck, T.
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    Hölck, O.
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    Hermann, S.
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    Schulz, S.E.
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    Gessner, T.
    ;
    Wunderle, B.
    To study the mechanical interface behavior of single-walled carbon nanotubes (CNTs) embedded in a noble metal, we performed CNTmetal pull-out tests with in situ scanning electron microscope experiments. Molecular dynamics (MD) simulations were conducted to predict forcedisplacement data during pull-out, providing critical forces for failure of the system. In MD simulations, we focused on the influence of carboxylic surface functional groups (SFGs) covalently linked to the CNT. Experimentally obtained maximum forces between 10 and 102 nN in palladium and gold matrices and simulated achievable pulling forces agree very well. The dominant failure mode in the experiment is CNT rupture, although several pull-out failures were also observed. We explain the huge scatter of experimental values with varying embedding length and SFG surface density. From simulation, we found that SFGs act as small anchors in the metal matrix and significantly enhance the maximum forces. This interface reinforcement can lead to tensile stresses sufficiently high to initiate CNT rupture. To qualify the existence of carboxylic SFGs on our CNT material, we performed analytical investigation by means of fluorescence labeling of surface species and discuss the results. With this contribution, we focus on a synergy between computational and experimental approaches involving MD simulations, nano scale testing, and analytics (1) to predict to a good degree of accuracy maximum pull-out forces of single-walled CNTs embedded in a noble metal matrix and (2) to provide valuable input to understand the underlying mechanisms of failure with focus on SFGs. This is of fundamental interest for the design of future mechanical sensors incorporating piezoresistive single-walled CNTs as the sensing element.
  • Publication
    Mikrofluidische Schnittstellen durch Laserstrukturierung
    ( 2008)
    Baum, M.
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    Keiper, B.
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    Hänel, J.
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    Otto, T.
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    Gessner, T.
  • Publication
    Micro machining technologies for non silicon materials
    ( 2008)
    Baum, M.
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    Rota, A.
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    Salk, N.
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    Otto, T.
    ;
    Gessner, T.
  • Publication
    enversys - Towards a Competence Center for Advanced Engineering and Verification Techniques for Heterogeneous Systems
    ( 2007)
    Specht, H.
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    Mehner, J.
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    Otto-Adamczak, T.
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    Cristiano, D.
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    Winkler, T.
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    Neugebauer, R.
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    Gessner, T.
  • Publication
    Wafer-Level Active Testing of Capacitive Inertial Sensors
    ( 2007)
    Nowack, M.
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    Reuter, D.
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    Rennau, M.
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    Bertz, A.
    ;
    Gessner, T.
  • Publication
  • Publication
    Investigation of bonding behaviour of different borosilicate glasses
    ( 2000)
    Wiemer, M.
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    Hiller, K.
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    Gessner, T.
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    Kloss, T.
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    Schneider, K.
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    Leipold-Haas, U.
    ;
    Bagdahn, J.
    ;
    Petzold, M.
    New investigations were carried out in order to characterise the anodic bonding behaviour of borosilicate glass Borofloat 33 in comparison with different suppliers of borosilicate glass wafers. Firstly the original surfaces were characterised. This was followed by anodic bonding experiments of the glass wafers with unpatterned and patterned silicon wafers. The compounds with unpatterned substrates were evaluated and compared with respect to the parameters bonding temperature, bonding time and current flow. Furthermore, test patterns (Chevron notches) for evaluation of bond strength were prepared, anodically bonded to the glass wafers and then loaded using the Micro Chevron Test up to the failure of the bond.