Verification of the master curve concept (ASTM E1921) and inhomogeneity analysis of a German RPV weld for various loading rates

Fracture-mechanical investigations were carried out on the weld metal of a German reactor pressure vessel steel 22NiMoCr3-7. The crack tip loading rate and test temperature were varied in the brittle-ductile transition region, while the results were evaluated using the Master Curve methodology (ASTM E1921), including inhomogeneity analyses in Appendix X5. The highly inhomogeneous datasets could be uniformly described with a bimodal distribution function with good accuracy compared to the standard procedure. However, this agreement decreases with increasing crack tip loading rate. In contrast, a modified Master Curve with a shape factor of p = 0.03 /°C progressively matches the data better with increasing crack tip loading rate. The weld metal has a significantly higher toughness than the base material. SEM analysis suggests that the inhomogeneity is due to the stochastic distribution of sharp microcracks, while the observed inhomogeneity is additionally superimposed by dynamic effects (adiabatic heating and local crack arrest) at increased crack tip loading rates. It is argued that the microstructural inhomogeneity is hereby »neutralized« and could instead be interpreted as a possible artifact of the standard Master Curve under dynamic conditions.