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  4. Accessing local electron-beam induced temperature changes during In situ liquid-phase transmission electron microscopy
 
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2021
Journal Article
Title

Accessing local electron-beam induced temperature changes during In situ liquid-phase transmission electron microscopy

Abstract
A significant electron-beam induced heating effect is demonstrated for liquid-phase transmission electron microscopy at low electron flux densities using Au nanoparticles as local nanothermometers. The obtained results are in agreement with theoretical considerations. Furthermore, the impact of beam-induced heating on radiolysis chemistry is estimated and the consequences of the effect are discussed.
Author(s)
Fritsch, B.
Electron Devices (LEB), Department of Electrical, Electronic and Communication Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Cauerstraße 6, Erlangen, 91058, Germany
Hutzler, A.
Electron Devices (LEB), Department of Electrical, Electronic and Communication Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Cauerstraße 6, Erlangen, 91058, Germany
Wu, M.
Institute of Micro- and Nanostructure Research (IMN), Center for Nanoanalysis and Electron Microscopy (CENEM), Interdisciplinary Center for Nanostructured Films (IZNF), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Cauerstraße 3, Erlangen, 91058, Germany
Khadivianazar, S.
Electron Devices (LEB), Department of Electrical, Electronic and Communication Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Cauerstraße 6, Erlangen, 91058, Germany
Vogl, L.
Institute of Micro- and Nanostructure Research (IMN), Center for Nanoanalysis and Electron Microscopy (CENEM), Interdisciplinary Center for Nanostructured Films (IZNF), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Cauerstraße 3, Erlangen, 91058, Germany
Jank, M.  
Fraunhofer-Institut für Integrierte Systeme und Bauelementetechnologie IISB  
März, M.  
Fraunhofer-Institut für Integrierte Systeme und Bauelementetechnologie IISB  
Spiecker, E.
Institute of Micro- and Nanostructure Research (IMN), Center for Nanoanalysis and Electron Microscopy (CENEM), Interdisciplinary Center for Nanostructured Films (IZNF), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Cauerstraße 3, Erlangen, 91058, Germany
Journal
Nanoscale advances  
Open Access
DOI
10.1039/D0NA01027H
Language
English
Fraunhofer-Institut für Integrierte Systeme und Bauelementetechnologie IISB  
Keyword(s)
  • electron beams

  • gold metallography

  • gold nanoparticles

  • high resolution transmission electron microscopy

  • radiation chemistry

  • transmission

  • Au nanoparticle

  • electron flux

  • induced heating

  • induced temperature

  • liquid phase

  • electron

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