X-ray microscopy and tomography of hydrogen storage materials

This paper is focused on the application of X-ray microscopy to study the change of the morphology of energy storage materials. A lab-based X-ray microscope (XCT, Carl Zeiss nano XCT 100) with a resolution better than 100 nm in the reconstructed volume is used for the experiments. The results are validated by experimental data obtained by scanning electron microscopy (SEM, Carl Zeiss NVision 40), transmission electron microscopy (TEM, Carl Zeiss LIBRA 200 Cs MC) and electron energy loss spectroscopy (EELS).