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  4. Energy density optimization in laser-based powder bed fusion of nano-modified PA12 powder feedstocks
 
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2025
Journal Article
Title

Energy density optimization in laser-based powder bed fusion of nano-modified PA12 powder feedstocks

Abstract
Additive manufacturing (AM) by powder bed fusion using a laser beam (PBF-LB) is often considered as the process of choice for industrial applications. Small changes in process parameters and intrinsic or extrinsic material parameters can significantly affect the final as-built part properties in this highly complex AM process. Choosing a machine configuration with optimal process parameters can be time-consuming, especially when new powders, i.e., nano-modified feedstocks or batches, are used. Even if a set of parameters works for one PBF-LB machine, the same parameters may produce unsatisfactory results on another machine model. Dimensionless parameters can be beneficial in simplifying complex phenomena. In this study, a semi-analytical approach based on printing monolayers was semi-blind tested by five laboratories on different PBF-LB machines. Virgin polyamide 12 (PA12), silver, and carbon black nano-particle-modified PA12 powders were tested. Two dimensionless numbers were used to describe the process. The first number describes the energy conversion dimensionless. The second dimensionless number proposes a minimum energy input demand for full densification. Both numbers combine process parameters (e.g., laser power, scan speed) and material properties (latent heat and solid density), while energy conversion number is considered by experimental results (monolayer thickness). Results indicate how nanoparticles influence thermal conductivity and energy absorption. Suggested surface energy densities based on the dimensionless numbers were compared with mechanical properties. The prediction of the highest overall mechanical values (tensile strength and elongation at break) matched the best mechanical properties. The monolayer approach presents an experimental simple method for predicting suitable machine settings and narrowing the process window in an efficient and material-conserving way.
Author(s)
Grünewald, Moritz
Fraunhofer-Institut für Produktionstechnik und Automatisierung IPA  
Ziefuss, Anna R.
Universität Duisburg-Essen
Schlör, Christian
SKZ - German Plastics Center
Popp, Kevin
SKZ - German Plastics Center
Gann, Stan
Universität Duisburg-Essen
Kusoglu, Ihsan Murat
Universität Duisburg-Essen
Barcikowski, Stephan
Universität Duisburg-Essen
Greiner, Joachim
Universität Stuttgart
Middendorf, Peter
Universität Stuttgart
Gruber, Piotr
Politechnika Wrocławska
Olejarczyk, Michał
Politechnika Wrocławska
Kurzynowski, Tomasz
Politechnika Wrocławska
Wang, Zhengze
Sichuan University
Huang, Yajiang
Sichuan University
Coskun, Mert
Fatih Sultan Mehmet Vakıf Üniversitesi
Kısasöz, Burçin Özbay
Fatih Sultan Mehmet Vakıf Üniversitesi
Koc, Ebubekir
Fatih Sultan Mehmet Vakıf Üniversitesi
Rudloff, Johannes
SKZ - German Plastics Center
Journal
Journal of Materials Science : JMS  
Open Access
DOI
10.1007/s10853-025-11128-6
Additional link
Full text
Language
English
Fraunhofer-Institut für Produktionstechnik und Automatisierung IPA  
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