Coupled microscopic and micromagnetic depth-specific analysis of plastic deformation and phase transformation of metastable austenitic steel AISI 304L by flow forming

This paper presents the characterization of the microstructure evolution during flow forming of austenitic stainless steel AISI 304L. Due to plastic deformation of metastable austenitic steel, phase transformation from γ-Austenite into α'-martensite occurs. This is initiated by the formation of shear bands as product of the external stresses. By means of coupled microscopic and micromagnetic investigations, a characterization of the microstructure was carried out. In particular, this study shows the distribution of the strain-induced α'-martensite and its influence on material properties like hardness at different depths. The microstructural analyses by means of electron backscattered diffraction (EBSD) technique, evidence a higher amount of α'-martensite (ca. 23 %) close to the outer specimen surface, where the plastic deformation and the direct contact with the forming tool take place. In the middle area (ca. 1.5 mm depth from the outer surface), the portion of transformed α'-martensite drops to 7 % and in the inner surface to 2 %. These results are well correlated with microhardness and micromagnetic measurements at different depths. EBSD and atomic force microscopy (AFM) were used to make a detailed characterization of the topography and degree of deformation of the shear bands. Likewise, the mechanisms of nucleation of α'-martensite were discussed. This research contributes to the development of micromagnetic sensors to monitor the evolution of properties during flow forming. This makes them more suitable for closed-loop property control, which offers possibilities for an application-oriented and more efficient production.