Now showing 1 - 8 of 8
  • Publication
    In situ microstructure analysis of Inconel 625 during laser powder bed fusion
    ( 2022)
    Schmeiser, Felix
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    Krohmer, Erwin
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    Wagner, Christian
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    Schell, Norbert
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    ;
    Reimers, Walter
    Laser powder bed fusion is an additive manufacturing process that employs highly focused laser radiation for selective melting of a metal powder bed. This process entails a complex heat flow and thermal management that results in characteristic, often highly textured microstructures, which lead to mechanical anisotropy. In this study, high-energy X-ray diffraction experiments were carried out to illuminate the formation and evolution of microstructural features during LPBF. The nickel-base alloy Inconel 625 was used for in situ experiments using a custom LPBF system designed for these investigations. The diffraction patterns yielded results regarding texture, lattice defects, recrystallization, and chemical segregation. A combination of high laser power and scanning speed results in a strong preferred crystallographic orientation, while low laser power and scanning speed showed no clear texture. The observation of a constant gauge volume revealed solid-state texture changes without remelting. They were related to in situ recrystallization processes caused by the repeated laser scanning. After recrystallization, the formation and growth of segregations were deduced from an increasing diffraction peak asymmetry and confirmed by ex situ scanning transmission electron microscopy.
  • Publication
    Internal Stress Evolution and Subsurface Phase Transformation in Titanium Parts Manufactured by Laser Powder Bed Fusion - An In Situ X-Ray Diffraction Study
    ( 2021)
    Schmeiser, Felix
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    Krohmer, Erwin
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    Schell, Norbert
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    ;
    Reimers, Walter
    Laser powder bed fusion (LPBF) is a metal additive manufacturing technology, which enables the manufacturing of complex geometries for various metals and alloys. Herein, parts made from commercially pure titanium are studied using in situ synchrotron radiation diffraction experiments. Both the phase transformation and the internal stress buildup are evaluated depending on the processing parameters. For this purpose, evaluation approaches for both temperature and internal stresses from in situ diffraction patterns are presented. Four different parameter sets with varying energy inputs and laser scanning strategies are investigated. A combination of a low laser power and scanning speed leads to a more homogeneous stress distribution in the observed gauge volumes. The results show that the phase transformation is triggered during the primary melting and solidification of the powder and subsurface layers. Furthermore, the stress buildup as a function of the part height during the manufacturing process is clarified. A stress maximum is formed below the part surface, extending into deeper layers with increasing laser power. A temperature evaluation approach for absolute internal stresses shows that directional stresses decrease sharply during laser impact and reach their previous magnitude again during cooling.
  • Publication
    Steuerung von Laser-induzierten periodischen Oberflächenstrukturen
    ( 2021) ;
    Souza Schweitzer, Luiz Guilherme De
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    Schneider, Peter
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    Michel, Andre
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    Laser-induzierte periodische Oberflächenstrukturen (LIPSS) weisen ein hohes Potenzial für Anwendungen in den Bereichen der Oberflächenfunktionalisierung auf. Die Steuerung der Richtung dieser Nanostrukturen kann nur durch Änderung der Laserpolarisation erfolgen. Auf dem Markt gibt es kein System zur automatischen Änderung der LIPSS-Orientierung. Für den industriellen Einsatz ist dies vom Vorteil, um Inhomogenität im Strukturverlauf zu vermeiden. In diesem Beitrag wird eine Systemlösung vorgestellt, indem die Steuerung der Richtung von Nanotexturen ermöglicht wird.
  • Publication
  • Publication
    Ex Situ Residual Stress Analysis of Chemical Vapor Deposited Diamond Coated Cutting Tools by Synchrotron X-Ray Diffraction in Transmission Geometry
    ( 2021)
    Hinzmann, Daniel
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    Böttcher, Katrin
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    Reimers, Walter
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    When machining difficult-to-cut, nonferrous materials, chemical vapor deposited (CVD) diamond-coated cutting tools are applied. The tools' favorable mechanical property profile is based on the hardness of the coating as well as the adaptability of the substrate. Nevertheless, the reproducibility of machining results and process stability are limited by insufficient coating adhesion. The resulting cutting tool failure is based on coating delamination initiated by crack development. By assessing residual stress as an influence of coating adhesion, an analysis of CVD diamond-coated tools is performed using synchrotron X-ray diffraction in transmission geometry. Investigation of a nanocrystalline and multilayer morphology on cobalt-based tungsten carbide (WC-Co) and a silicon nitride-based ceramic (Si3N4) provides the distribution of the principal in-plane residual stress tensor component s22 depending on the coating morphology and substrate material. Contrary to microcrystalline CVD diamond, nanocrystalline layers decrease the compressive residual stress. In addition, the CVD diamond coating deposited on the Si3N4 substrate material tends to induce an overall initial tensile residual stress that leads to increased tool performance compared to WC-Co-based coated tools. Variation of the coating morphology as well as the substrate material offers the possibility to extend the current model for residual stress-dependent tool failure.
  • Publication
    In-Situ-Kraftmessung bei variablen Werkzeugwinkeln
    ( 2019) ;
    Uhlemann, Sebastian
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    Werkzeugentwicklungen sind von iterativen Anpassungen und aufwendigen Versuchsreihen mit einer Vielzahl von Prototypen geprägt. In einem Forschungsprojekt wurde ein sensorisch instrumentiertes Fräswerkzeug mit verstellbaren Schneiden entwickelt und mittels SLM (Selective Laser Melting) aufgebaut. Mit dieser Entwicklung liegt ein Instrument vor, das im Fräsprozess unmittelbar an den Schneiden Belastungen erfassen kann und durch nachgestellte FEM (Finite Elemente Methode)-Analysen und Optimierungsroutinen ein enormes Potenzial für die Auslegung optimierter Werkzeuggeometrien bietet.