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  4. Synthesis of novel bisphosphorylimides based on Staudinger reaction
 
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2020
Journal Article
Title

Synthesis of novel bisphosphorylimides based on Staudinger reaction

Abstract
A series of bisphosphorylimides based on the reaction sequence of Atherton-Todd and Staudinger reaction were synthesized. These bisphosphorylimides containing phosphorus in different chemical environments, while the reaction sequence is using mild conditions and more over can be synthesized in an one-pot procedure. The molecular structures were revealed by nuclear magnetic resonance spectroscopy and x-ray crystallography. The stability of the bisphosphorylimides against hydrolysis and thermal influences was tested which allows an initial estimation about the usage as flame retardant.
Author(s)
Weber, Lais  
Fraunhofer-Institut für Betriebsfestigkeit und Systemzuverlässigkeit LBF  
Weinert, Michael  orcid-logo
Fraunhofer-Institut für Chemische Technologie ICT  
Goedderz, Daniela  
Fraunhofer-Institut für Betriebsfestigkeit und Systemzuverlässigkeit LBF  
Fuhr, Olaf
Institute of Nanotechnology (INT) and Karlsruhe Nano Micro Facility (KNMF)
Döring, Manfred
Fraunhofer-Institut für Betriebsfestigkeit und Systemzuverlässigkeit LBF  
Journal
Arkivoc  
Open Access
File(s)
Download (1.8 MB)
Rights
CC BY 4.0: Creative Commons Attribution
DOI
10.24406/publica-r-262331
10.24820/ark.5550190.p011.150
Language
English
Fraunhofer-Institut für Chemische Technologie ICT  
Fraunhofer-Institut für Betriebsfestigkeit und Systemzuverlässigkeit LBF  
Keyword(s)
  • 9,10-Dihydro-9-oxa-10-phosphaphenanthrene-10-oxide

  • phosphorus

  • bisphosphorylimides

  • Staudinger reaction

  • Atherton-Todd reaction

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