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Development of an HPLC-NMR method for the determination of PAHs in soil samples

A comparison with conventional methods
: Weißhoff, H.; Preiß, A.; Nehls, I.; Win, T.; Mügge, C.


Analytical and bioanalytical chemistry 373 (2002), Nr.8, S.810-819
ISSN: 1618-2642 (Print)
ISSN: 1618-2650 (Online)
Fraunhofer ITA ( ITEM) ()
hyphenated technique; high performance liquid chromatography; polycyclic aromatic hydrocarbon; soil chemistry; environmental chemistry; methodology

A hyphenated HPLC-1H NMR method for the identification and quantification of PAHs in soil samples has been developed and applied to a PAH reference sample provided by the Federal Institute for Materials Research and Testing (BAM, Berlin, Germany). The results were compared with those obtained by HPLC-DAD, HPLC-F, and GC-MS analyses of the same sample.