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  4. Non-isothermal kinetics of high temperature oxidation studied by a fast X-ray diffraction method.
 
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1992
Journal Article
Title

Non-isothermal kinetics of high temperature oxidation studied by a fast X-ray diffraction method.

Other Title
Untersuchung der nichtisothermen Kinetik der Hochtemperatur-Oxidation mittels schneller Röntgenbeugung
Abstract
Temperature resolved X-ray diffraction using a diffractometer equipped with a high temperature device was applied to the study of the oxidation of Fe-ARMCO below 570 degree C. The oxidation products are identified in situ and the difference method yields curves Y(T) showing the global changes. These curves were calibrated to the microscopically measured and thickness of the oxide layer obtaining the growth x(T). A calculated curve including the Arrhenius relation was fitted to the x(T) curve yielding activation energy and values of the oxidation rate constant as a function of temperature.
Author(s)
Kolarik, Vladislav  
Eisenreich, N.
Engel, W.
Juez-Lorenzo, Maria del Mar  
Journal
Journal of thermal analysis  
DOI
10.1007/BF01979393
Language
English
Fraunhofer-Institut für Chemische Technologie ICT  
Keyword(s)
  • Armco iron

  • corrosion

  • high temperature oxidation

  • in situ investigation

  • non-isothermal kinetics

  • oxidation product

  • x-ray diffraction

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