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Development of a Simple Setup for Temperature Dependent Mass Spectrometric Measurements for the Investigation of Outgassing Effects in Polymeric Materials for Solar Application

: Piekarczyk, Andreas; Heitmann, Ulrike; Weiß, Karl-Anders; Köhl, Michael; Bald, Ilko

Fulltext urn:nbn:de:0011-n-5782211 (1.7 MByte PDF)
MD5 Fingerprint: 80fac3aa621392fe7a196630af74b653
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Created on: 15.10.2020

Polymer testing 81 (2020), Art. 106164, 8 pp.
ISSN: 0142-9418
European Commission EC
FP7-ENERGY - Revisiting solar-thermal systems for using breakthroughs in scientific and technological fields; 282638; SCOOP
Solar Collectors made of Polymers
Journal Article, Electronic Publication
Fraunhofer ISE ()
energieeffizientes Gebäude; Lüftungs- und Klimatechnik

A simple experimental setup for temperature dependent mass spectrometric measurements has been constructed. It consists of a heated sample chamber and a mass spectrometer and allows for measurements under inert gas and ambient air. Based on initial measurements on two extruded polystyrene (XPS) samples a methodology for the data analysis has been developed. With this methodology the outgassing temperature of volatile compounds, which were used as blowing agents, has been identified. Furthermore, the composition of the blowing agents has been analyzed by temperature dependent mass spectra. The results indicate the use of ambient air in one material and a mixture of the banned blowing agents R142b and R22, both hydrochlorofluorocarbons (HCFC), in the other material. The here described methodology provides an easy to use approach to identify such compounds, for example as part of environmental or quality control.