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2006
Journal Article
Title
Densification of liquid phase sintered silicon carbide
Other Title
Verdichtung von flüssigphase-gesintertem Siliciumcarbid
Abstract
The densification and phase formation of liquid phase sintered silicon carbide (LPSSiC) with 10wt.% additives were investigated. The ratio of the Al(sub 2)O(sub 3)/Y(sub 2)O(sub 3)-additives was changed between 4:1 and 1:2. Densification was carried out by hot pressing and gas pressure sintering. The different densification routes result in different major grain boundary phases-aluminates in gas pressure sintered materials and silicates in hot pressed samples. Thermodynamic calculations were carried out to determine the amount of liquid phase during densification and for the interpretation of the results.
Keyword(s)
additives
ceramic
densification
grain boundary
hot-pressing
silicon compound
sintering
thermodynamics
Siliciumcarbid
Flüssigphasensintern
Zusatzstoff
Aluminiumoxid
Yttriumoxid
Mullit
Yttriumaluminiumgranat
Mikrogefüge
Verdichtung
Heißpressen
Gasdrucksintern
Korngrenze
flüssige Phase
Thermodynamik
Dichte
Masse
Phasendiagramm
Röntgenbeugung
energiedispersive Röntgenspektrometrie (EDXS)